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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 131726Generated: November 1, 2026

Methyl iodide → HCID 10115801, compound

https://huagongshe.com/reaction/131726

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl iodideHCID 6328—
ReactantHCID 10114893HCID 10114893—
ProductHCID 10115801HCID 10115801—

Reaction Steps

2′-Methyl-N-methyl-5′-(5-methyl-1,3,4-oxadiazol-2-yl)-N-(2-trifluoromethylbenzyl)-1,1′-biphenyl-4-carboxamide was prepared from 2′-methyl-5′-(5-methyl-1,3,4-oxadiazol-2-yl)-N-(2-trifluoromethylbenzyl)-1,1′-biphenyl-4-carboxamide and iodomethane using method L. NMR; δH [2H6]—DMSO 7.90,(1H, d), 7.80-7.51,(9H, m), 7.41,(1H, b), 4.89-4.71,(2H, m), 3.01-2.96,(3H, m), 2.56,(3H, s), 2.33-2.24,(3H, m). LCMS; retention time 3.62 min, MH+ 466.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07384963B2
Source datasetuspto-grants-2008_06
ORD IDord-41a6ffd0ccff4aa3be637190ed5b6bf4
Source noteuspto-grants-2008_06