4-[2-methyl-5-(5-methyl-1,3,4-oxadiazol-2-yl)phenyl]benzoic Acid → HCID 10187182, compound

HRID 131734Notes

Reaction equation

HRID 131734 reaction equation
[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[O:9][C:10]([CH3:13])=[N:11][N:12]=2)=[CH:4][C:3]=1[C:14]1[CH:19]=[CH:18][C:17]([C:20](O)=[O:21])=[CH:16][CH:15]=1.[NH2:23][C:24]1[CH:40]=[CH:39][C:27]([O:28][C:29]2[CH:34]=[CH:33][C:32]([S:35]([NH2:38])(=[O:37])=[O:36])=[CH:31][CH:30]=2)=[CH:26][CH:25]=1>>[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[O:9][C:10]([CH3:13])=[N:11][N:12]=2)=[CH:4][C:3]=1[C:14]1[CH:15]=[CH:16][C:17]([C:20]([NH:23][C:24]2[CH:40]=[CH:39][C:27]([O:28][C:29]3[CH:34]=[CH:33][C:32]([S:35](=[O:37])(=[O:36])[NH2:38])=[CH:31][CH:30]=3)=[CH:26][CH:25]=2)=[O:21])=[CH:18][CH:19]=1

Participants

3

Reactant 2

HCID 112201194-[2-methyl-5-(5-methyl-1,3,4-oxadiazol-2-yl)phenyl]benzoic AcidHCID 50989672108016-36-0

Product 1

HCID 10187182HCID 10187182, compound

Procedure

2′-Methyl-5′-(5-methyl-1,3,4-oxadiazol-2-yl)-N-[4-(4-sulphamoylphenoxy)phenyl-]1,1′-biphenyl-4-carboxamide was prepared from 2′-methyl-5′-(5-methyl-1,3,4-oxadiazol-2-yl)-1,1′-biphenyl-4-carboxylic acid and 4-(4-aminophenoxy)phenylsulphonamide using method I. LCMS; retention time 3.38 min, MH+ 541.

Sources & evidence

ORD record
ord-357a58471c39402db4e378e5d4b4577b
Source dataset
uspto-grants-2008_06
Patent number
US07384963B2

Reaction notes

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