HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67462948, compound → HCID 67462066, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67462948 | HCID 67462948 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 67462066 | HCID 67462066 | — |
Reaction Steps
To a solution of 4-[1-(3-methoxy-4-benzyloxyphenacyl)-1H-benzimidazol-2-yl]-furazan-3-ylamine (1.00 g) in THF (20 ml) is added palladium on carbon (10%, 0.2 g). The mixture is stirred under a hydrogen atmosphere for 1 hour. The catalyst is filtered and the filtrate is evaporated to dryness to give the title compound in pure form, m.p. 265° C. (This compound is also listed as Example 74 in Table 1.)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07385061B2 |
| Source dataset | uspto-grants-2008_06 |
| ORD ID | ord-d2a1f9772dbf495aa97be93ea5b6a054 |
| Source note | uspto-grants-2008_06 |