Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 132015Generated: October 29, 2026

HCID 67462948, compound → HCID 67462066, compound

https://huagongshe.com/reaction/132015

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 67462948HCID 67462948—
CatalystPalladiumHCID 23938—
SolventTetrahydrofuranHCID 8028—
ProductHCID 67462066HCID 67462066—

Reaction Steps

To a solution of 4-[1-(3-methoxy-4-benzyloxyphenacyl)-1H-benzimidazol-2-yl]-furazan-3-ylamine (1.00 g) in THF (20 ml) is added palladium on carbon (10%, 0.2 g). The mixture is stirred under a hydrogen atmosphere for 1 hour. The catalyst is filtered and the filtrate is evaporated to dryness to give the title compound in pure form, m.p. 265° C. (This compound is also listed as Example 74 in Table 1.)

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07385061B2
Source datasetuspto-grants-2008_06
ORD IDord-d2a1f9772dbf495aa97be93ea5b6a054
Source noteuspto-grants-2008_06