HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formic Acid → 1,2-Octanediol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formic Acid | HCID 284 | — |
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | 1-Octene | HCID 8125 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 1,2-Octanediol | HCID 14231 | — |
Reaction Steps
314 g (2.80 mol) of 1-octene were reacted with 330 g (7.17 mol) of formic acid and 232 g (3.41 mol) of a 50% strength aqueous H2O2 solution in accordance with Example 4. 575 g of ethanol were employed for the Marlon AS3 acid-catalyzed transesterification, and the main fraction obtained after the workup by distillation was >99.5% pure, virtually odorless 1,2-octanediol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07385092B2 |
| Source dataset | uspto-grants-2008_06 |
| ORD ID | ord-8b5bfc5c2e4f4207b96cac42383d4bc7 |
| Source note | uspto-grants-2008_06 |