4-Nitrosoprocainamide → 4-Nitrosoprocainamide

HRID 132507Notes

Reaction equation

HRID 132507 reaction equation
[CH3:1][CH2:2][N:3]([CH2:6][CH2:7][NH:8][C:9]([C:11]1[CH:16]=[CH:15][C:14]([N:17]=[O:18])=[CH:13][CH:12]=1)=[O:10])[CH2:4][CH3:5]>O>[CH3:5][CH2:4][N:3]([CH2:6][CH2:7][NH:8][C:9]([C:11]1[CH:16]=[CH:15][C:14]([N:17]=[O:18])=[CH:13][CH:12]=1)=[O:10])[CH2:2][CH3:1].[OH2:10].[CH3:5][CH2:4][N:3]([CH2:6][CH2:7][NH:8][C:9]([C:11]1[CH:16]=[CH:15][C:14]([N:17]=[O:18])=[CH:13][CH:12]=1)=[O:10])[CH2:2][CH3:1]

Participants

4

Reactant 1

HCID 1256014-Nitrosoprocainamide

Product 2

HCID 1256014-NitrosoprocainamideHCID 131726924HCID 131726924, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent2×

Procedure

The NOPA/water slurry was prepared by dispersing NOPA crystals in water under ambient conditions, and by oven-annealing the slurry in a closed container at a temperature of 70° C. for a time sufficient so as to yield a pourable, translucent, partial-solution of NOPA in water. NOPA was similarly mixed with IPA to yield a completely soluble solution at room temperature. The octanoic acid and NOS compounds were used as received in their neat liquid forms.

Sources & evidence

ORD record
ord-0fc1fdf047c040b8a9ed9c3b8ce2627f
Source dataset
uspto-grants-2008_06
Patent number
US07387795B2

Reaction notes

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