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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 132691Generated: October 30, 2026

Pyridine → HCID 24967317, compound

https://huagongshe.com/reaction/132691

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPyridineHCID 1049—
ReactantHCID 86600502HCID 86600502—
SolventTetrahydrofuranHCID 8028—
ProductHCID 24967317HCID 2496731766.4%

Reaction Steps

To a plastic vial containing compound 3B (20 mg, 0.041 mmol) in 0.2 mL of THF was added 100 μL of HF pyridine solution (Aldrich), and stirred at RT overnight. It was concentracted and purified on prepHPLC to give the title compound (10.2 mg). MS (ES) m/z 375 [M+H]+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07388027B2
Source datasetuspto-grants-2008_06
ORD IDord-4a10d855865c4aeda38ed31cc3e6ab56
Source noteuspto-grants-2008_06