HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 24967317, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | HCID 86600502 | HCID 86600502 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 24967317 | HCID 24967317 | 66.4% |
Reaction Steps
To a plastic vial containing compound 3B (20 mg, 0.041 mmol) in 0.2 mL of THF was added 100 μL of HF pyridine solution (Aldrich), and stirred at RT overnight. It was concentracted and purified on prepHPLC to give the title compound (10.2 mg). MS (ES) m/z 375 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07388027B2 |
| Source dataset | uspto-grants-2008_06 |
| ORD ID | ord-4a10d855865c4aeda38ed31cc3e6ab56 |
| Source note | uspto-grants-2008_06 |