HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 23125820, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | 2,3-Di(propan-2-yl)butane-1,4-diol | HCID 23126029 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 23125820 | HCID 23125820 | 87% |
Reaction Steps
7.7 g 2,3-diisopropyl-1,4-butandiol and 100 ml THF were mixed, and to the mixture was added 12.5 g benzoyl chloride and 14 g pyridine. The mixture was heated refluxing for 4 hours. Upon completing the reaction, water was added to dissolve solid substance. The organic phase was separated, washed, dried, and concentrated to give 13.9 g product, and the yield was 87%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07388061B2 |
| Source dataset | uspto-grants-2008_06 |
| ORD ID | ord-7b0ccd0fa38a4908bf56559c6a7dd751 |
| Source note | uspto-grants-2008_06 |