HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → HCID 69204603, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | HCID 67562678 | HCID 67562678 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 69204603 | HCID 69204603 | — |
Reaction Steps
BOC-Protected aminodiol 28 was dissolved in dichloromethane with tritethyamine and cooled to 0°. Benzoylchloride (1.0 eq.) was added and the solution stirred until all of the starting material was consumed. After extraction, the benzoyl ester (29) was purified using silica gel chromatography.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07388118B2 |
| Source dataset | uspto-grants-2008_06 |
| ORD ID | ord-67cefef253604c298495f5a41d9d3076 |
| Source note | uspto-grants-2008_06 |