HRID13293

反应详情

EQUATION

反应方程式

HRID 13293 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

20 mg of developed Raney nickel catalyst was added to a methanol (5 ml) solution of 161 mg of 5-(2-cyano-phenoxy)-4-(6-methanesulfonyl-pyridin-3-yloxy)-2-nitro-phenylamine obtained in (step 4), and the reaction liquid was stirred overnight in a hydrogen atmosphere. The catalyst was removed through filtration, and the solvent was evaporated away under reduced pressure to obtain the entitled compound.

WORKUP

后处理

  1. customobtained in (step 4)
  2. customthe reaction liquid
  3. customThe catalyst was removed through filtration
  4. customthe solvent was evaporated away under reduced pressure
  5. customto obtain the entitled compound