HRID133071

反应详情

EQUATION

反应方程式

HRID 133071 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A mixture of 50 mg (0.15 mmol) of tert-butyl 8-(cyclopropylmethylene)-2-(trifluoromethyl)-5,6-dihydro[1,2,4]triazolo[1,5-α]pyrazine-7(8H)-carboxylate and 25 mg of 10% palladium on carbon in 0.5 mL of ethanol was stirred under an atmosphere of hydrogen overnight. The mixture was filtered and the filtrate concentrated to give the title compound.

WORKUP

后处理

  1. filtrationThe mixture was filtered
  2. concentrationthe filtrate concentrated