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HRID133263

反应详情

EQUATION

反应方程式

HRID 133263 的结构方程式

REACTANTS

反应物

2
结构：CC(C)CI
HCID10556

Propane, 1-iodo-2-methyl-

C4H9I

结构：O=C1CC(=O)Nc2ccccc2N1
HCID283534

1H-1,5-Benzodiazepine-2,4(3H,5H)-dione

C9H8N2O2

PRODUCTS

生成物

1
结构：CC(C)CN1C(=O)CC(=O)N(CC(C)C)c2ccccc21
HCID22312768

未命名化合物

PROCEDURE

实验过程

2,4-Dioxo-1,5-bis-(2-methylpropyl)-2,3,4,5-tetrahydro-1H-1,5-benzodiazepine was prepared following General Procedure 8-M using the product from Example 8-P, Step A and 1-iodo-2-methylpropane (Aldrich). Purification was by flash chromatography eluting with EtOAc/hexanes (3:7 gradient to 1:1), then recrystallization from EtOAc/hexanes.

WORKUP

后处理

  1. customPurification
  2. washeluting with EtOAc/hexanes (3:7 gradient to 1:1)
  3. customrecrystallization from EtOAc/hexanes