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HRID133277

反应详情

EQUATION

反应方程式

HRID 133277 的结构方程式

REACTANTS

反应物

2
结构：O=C(O)C(O)c1cc(F)cc(F)c1
HCID588648

3,5-Difluoromandelic acid

C8H6F2O3

结构：C[C@H](N)C(=O)NC1N=C(c2ccccc2)c2ccccc2N(C)C1=O
HCID23552762

未命名化合物

PRODUCTS

生成物

1
结构：C[C@H](NC(=O)C(O)c1cc(F)cc(F)c1)C(=O)NC1N=C(c2ccccc2)c2ccccc2N(C)C1=O
HCID22984126

未命名化合物

PROCEDURE

实验过程

Following General Procedure D above using 3,5-difluoromandelic acid (Fluorochem) and 3-(L-alaninyl)amino-2,3-dihydro-1-methyl-5-phenyl-1H-1,4-benzodiazepin-2-one (Example 8-B), the title compound was prepared as a solid. The product was purified by LC 2000 chromatography, eluting with hexanes/ethyl acetate (20:80).

WORKUP

后处理

  1. customThe product was purified by LC 2000 chromatography
  2. washeluting with hexanes/ethyl acetate (20:80)