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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 133281Generated: October 30, 2026

3,5-Difluorophenylacetic acid → HCID 22984068, compound

https://huagongshe.com/reaction/133281

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3,5-Difluorophenylacetic acidHCID 145424—
ReactantHCID 23552783HCID 23552783—
ProductHCID 22984068HCID 22984068—

Reaction Steps

Following General Procedure D above using 3,5-difluorophenylacetic acid (Oakwood Products, Inc.) and 3-(L-alaninyl)amino-2,3-dihydro-1-isopropyl-5-phenyl-1H-1,4-benzodiazepin-2-one (Example 8-L), the title compound was prepared as a solid (mp.=208-209° C.). The product was purified by slurrying in ether/hexanes (1:1).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07390801B2
Source datasetuspto-grants-2008_06
ORD IDord-179c9b978d224b9bae4cce501e791a5b
Source noteuspto-grants-2008_06