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HRID133323

反应详情

EQUATION

反应方程式

HRID 133323 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)OC(=O)CBr
HCID79177

Acetic acid, bromo-, 1,1-dimethylethyl ester

C6H11BrO2

结构：C[C@H](Nc1ccc(Cl)c(Cl)c1)C(=O)O
HCID5491659

N-(3,4-Dichlorophenyl)alanine

C9H9Cl2NO2

PRODUCTS

生成物

1
结构：C[C@H](Nc1ccc(Cl)c(Cl)c1)C(=O)OCC(=O)OC(C)(C)C
HCID54406316

未命名化合物

PROCEDURE

实验过程

Following General Procedure AE above and using N-(3,4-dichlorophenyl)alanine (from Example AB above) and tert-butyl bromoacetate (Aldrich), the title compound was prepared as a solid. The reaction was monitored by silica gel tlc (Rf=0.57 in 25% EtOAc/hexanes). Purification was by recrystallization from ethanol.

WORKUP

后处理

  1. customPurification
  2. customwas by recrystallization from ethanol