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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 133358Erstellt: 25. Oktober 2026

L-Alanine → N-[(2-naphthyl)acetyl]-L-alanine Iso-butyl Ester

https://huagongshe.com/reaction/133358

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktL-AlanineHCID 5950—
Edukt2-Naphthaleneacetic acidHCID 11393—
ProduktN-[(2-naphthyl)acetyl]-L-alanine Iso-butyl EsterHCID 15481768—

Reaktionsschritte

Following General Procedure BB and using 2-naphthylacetic acid (Aldrich) and L-alanine is iso-butyl ester hydrochloride (from Example BB above), the title compound was prepared as a solid having a melting point of 128°-129° C. The reaction was monitored by tlc on silica gel and purification was by extraction with Et2O followed by washes with aqueous K2CO3 and aqueous HCl.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07390801B2
Quelldatensatzuspto-grants-2008_06
ORD IDord-b6ffa61a8c7b4a9cb5f26d2206c05357
Quellennotizuspto-grants-2008_06