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HRID133473

反应详情

EQUATION

反应方程式

HRID 133473 的结构方程式

REACTANTS

反应物

2
结构：CS(=O)(=O)CC(=O)c1ccccc1
HCID19457

Acetophenone, 2-(methylsulfonyl)-

C9H10O3S

结构：C[C@H](N)[C@@H](Cc1ccc(Cl)cc1)c1cccc(C#N)c1.Cl
HCID69268026

未命名化合物

PRODUCTS

生成物

1
结构：C[C@H](NC(CS(C)(=O)=O)c1ccccc1)[C@@H](Cc1ccc(Cl)cc1)c1cccc(C#N)c1
HCID11317292

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 3-(4-chlorophenyl)-2(S)(3-cyanophenyl)-1(S)-methyl-propylamine hydrochloride and 2-methanesulfonylacetophenone by the procedure of Example 33 as a mixture of two diastereomers. LC-MS: m/e=467 (M+1), 469 (M+3) (3.05 min and 4.05 min).

WORKUP

后处理

  1. customm/e=467 (M+1), 469 (M+3) (3.05 min and 4.05 min)