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HRID133741

反应详情

EQUATION

反应方程式

HRID 133741 的结构方程式

REACTANTS

反应物

2
结构：O=[N+]([O-])c1ccc(O)cc1F
HCID520948

3-Fluoro-4-nitrophenol

C6H4FNO3

结构：Cc1cc(NC(=O)C2(C)CO2)ccc1[N+](=O)[O-]
HCID71420003

2-Methyl-N-(3-methyl-4-nitrophenyl)oxirane-2-carboxamide

C11H12N2O4

PRODUCTS

生成物

1
结构：Cc1cc(NC(=O)C(C)(O)COc2ccc([N+](=O)[O-])c(F)c2)ccc1[N+](=O)[O-]
HCID86612737

未命名化合物

PROCEDURE

实验过程

3-(3-Fluoro-4-nitrophenoxy)-2-hydroxy-2-methyl-N-(3-methyl-4-nitrophenyl)propionamide was prepared as described in Example 1 starting from 3-fluoro-4-nitrophenol and 2-methyl-oxirane-2-carboxylic acid (3-methyl-4-nitrophenyl)amide. 1H NMR (DMSO-d6): 1.46 (3H, s), 2.53 (3H, s), 4.16 (1H, d, J=10.1 Hz), 4.41 (1H, d, J=10.1 Hz), 6.36 (1H, bs), 6.96 (1H, m), 7.22 (1H, m), 7.88 (1H, dd, J=9.0 Hz and 2.1 Hz), 7.90 (1H, d, J=2.1 Hz), 8.04 (1H, d, J=9.0 Hz), 8.24 (1H, m), 10.19 (1H, s).