HRID1348664

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：CC[C@H]1Oc2ccc(F)cc2N(CC(F)(F)F)C(=O)[C@H]1N(Cc1ccccc1)Cc1ccccc1

HCID21091452

未命名化合物

PRODUCTS

生成物

结构：CC[C@H]1Oc2ccc(F)cc2N(CC(F)(F)F)C(=O)[C@H]1N

HCID21091446

未命名化合物

收率 66%

AUXILIARIES

试剂、催化剂与溶剂

催化剂HCID23938

Palladium

溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

The title compound was prepared in 66% yield by hydrogenation of (6R,7S)-7-dibenzylamino-6-ethyl-2-fluoro-9-(2,2,2-trifluoro-ethyl)-6,7-dihydro-9H-5-oxa-9-aza-benzocyclohepten-8-one in methanol with Pd/C (10%), MS m/e (%): 307.1 (M+H+, 100).