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Dimethylamine → 4-dimethylaminomethyl-2-isobutyl-6-phenyl-2H-pyridazin-3-one
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dimethylamine | HCID 674 | — |
| 反応物 | 2-isobutyl-4-methanesulfonyloxymethyl-6-phenyl-2H-pyridazin-3-one | HCID 21991562 | — |
| 生成物 | 4-dimethylaminomethyl-2-isobutyl-6-phenyl-2H-pyridazin-3-one | HCID 21991586 | 81.1% |
反応手順
Following the procedure of Example 7, 2-isobutyl-4-methanesulfonyloxymethyl-6-phenyl-2H-pyridazin-3-one and dimethylamine were reacted to yield the title compound as a yellow oil (yield: 81.1%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07211577B2 |
| 出典データセット | uspto-grants-2007_05 |
| ORD ID | ord-18ffde3e4f084cbf9f2c962178507238 |
| 出典メモ | uspto-grants-2007_05 |