Dimethylamine → HCID 23018240, compound

HRID 1348753Notes

Reaction equation

HRID 1348753 reaction equation
[CH:1]1([CH2:4][N:5]2[C:10](=[O:11])[C:9]([CH2:12]OS(C)(=O)=O)=[CH:8][C:7]([C:18]3[CH:23]=[CH:22][C:21]([S:24]([CH3:27])(=[O:26])=[O:25])=[CH:20][CH:19]=3)=[N:6]2)[CH2:3][CH2:2]1.[CH3:28][NH:29][CH3:30]>>[CH:1]1([CH2:4][N:5]2[C:10](=[O:11])[C:9]([CH2:12][N:29]([CH3:30])[CH3:28])=[CH:8][C:7]([C:18]3[CH:23]=[CH:22][C:21]([S:24]([CH3:27])(=[O:26])=[O:25])=[CH:20][CH:19]=3)=[N:6]2)[CH2:3][CH2:2]1

Participants

3

Reactant 2

HCID 674DimethylamineHCID 219916462-cyclopropylmethyl-4-methanesulfonyloxymethyl-6-[4-(methyl-sulfonyl)phenyl]-2H-pyridazin-3-one

Product 1

HCID 23018240HCID 23018240, compoundYield 65.6%

Procedure

Following the procedure of Example 1(10), 2-cyclopropylmethyl-4-methanesulfonyloxymethyl-6-[4-(methylsulfonyl)phenyl]-2H-pyridazin-3-one and dimethylamine were reacted to yield the title compound as a yellow oil (yield: 65.6%).

Workup

  1. customwere reacted

Sources & evidence

ORD record
ord-177b91478d5a482797fc5ca09a9d3f7e
Source dataset
uspto-grants-2007_05
Patent number
US07211577B2

Reaction notes

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