HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorophenethyl mesylate → HCID 22562288, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorophenethyl mesylate | HCID 12942078 | — |
| Reactant | 6-(4-fluoro-3-methylphenyl)-4-methoxycarbonyl-2H-pyridazin-3-one | HCID 21991459 | — |
| Product | HCID 22562288 | HCID 22562288 | 56.3% |
Reaction Steps
Following the procedure of Example 1(6), 6-(4-fluoro-3-methylphenyl)-4-methoxycarbonyl-2H-pyridazin-3-one and 2-(4-chlorophenyl)ethanol methanesulfonate were reacted to yield a crude product. Without purification, the crude product was reacted further in accordance with the procedure of Example 1 (7) to yield the title compound as a pale yellow solid (yield: 56.3%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07211577B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-91acfb431fc34f0d8bf33e772f99b426 |
| Source note | uspto-grants-2007_05 |