HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(2-Chlorophenyl)-1-propanol methanesulfonate → HCID 23102901, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(2-Chlorophenyl)-1-propanol methanesulfonate | HCID 19688448 | — |
| Reactant | 6-(3-fluoro-4-methoxyphenyl)-4-methoxycarbonyl-2H-pyridazin-3-one | HCID 21991432 | — |
| Product | HCID 23102901 | HCID 23102901 | 56% |
Reaction Steps
Following the procedure of Example 1(6), 6-(3-fluoro-4-methoxyphenyl)-4-methoxycarbonyl-2H-pyridazin-3-one and 3-(2-chlorophenyl)-1-propanol methanesulfonate were reacted to yield a crude product. Without purification, the crude product was reacted further in accordance with the procedure of Example 1 (7) to yield the title compound as a pale yellow solid (yield: 56.0%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07211577B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-2364a0b2257b490dae72de0691e9e12c |
| Source note | uspto-grants-2007_05 |