HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(4-Chloro-2-nitrophenyl)-1,3,4-thiadiazole-2-sulfonyl chloride → N-{2-[5-(4-chloro-2-nitrophenyl)-1,3,4-thiadiazole-2-sulfonylamino]-ethyl}-glycine ethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(4-Chloro-2-nitrophenyl)-1,3,4-thiadiazole-2-sulfonyl chloride | HCID 21092751 | — |
| Reactant | N-beta-Aminoethyl-gly-oet 2hcl | HCID 74889816 | — |
| Product | N-{2-[5-(4-chloro-2-nitrophenyl)-1,3,4-thiadiazole-2-sulfonylamino]-ethyl}-glycine ethyl ester | HCID 21092774 | — |
Reaction Steps
The title compound was synthesized by the reaction of N-(2-aminoethyl)-glycine ethyl ester 2HCl with 5-(4-chloro-2-nitrophenyl)-1,3,4-thiadiazole-2-sulfonyl chloride as per the procedure of example 1. 1H NMR (500 MHz; DMSO-d6) δ 8.40 (d, 1H), 8.05 (dd, 1H), 8.02 (d, 1H) 4.07 (q, 2H), 3.30 (s, 2H), 3.19 (t, 2H), 2.67 (t, 2H), 1.18 (t, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07211668B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-098c90b97d66462e99ebf94bc97cd214 |
| Source note | uspto-grants-2007_05 |