HCID 10198095, compound → HCID 21092805, compound

HRID 1348968Notes

Reaction equation

HRID 1348968 reaction equation
Cl.Cl.[CH2:3]([O:5][C:6](=[O:12])[CH2:7][NH:8][CH2:9][CH2:10][NH2:11])[CH3:4].[CH3:13][C:14]1[S:18][C:17]([S:19](Cl)(=[O:21])=[O:20])=[N:16][N:15]=1>>[CH2:3]([O:5][C:6](=[O:12])[CH2:7][NH:8][CH2:9][CH2:10][NH:11][S:19]([C:17]1[S:18][C:14]([CH3:13])=[N:15][N:16]=1)(=[O:21])=[O:20])[CH3:4]

Participants

3

Reactant 2

HCID 10198095HCID 10198095, compoundHCID 74889816N-beta-Aminoethyl-gly-oet 2hcl

Product 1

HCID 21092805HCID 21092805, compound

Procedure

The title compound was synthesized by the reaction of N-(2-aminoethyl)-glycine ethyl ester 2HCl with 5-methyl-1,3,4-thiadiazole-2-sulfonyl chloride as per the procedure of example 1. 1H HMR (500 MHz; DMSO-d6) δ 4.07 (q, 2H), 3.27 (s, 2H), 3.09 (t, 2H), 2.82 (s, 3H), 2.62 (t, 2H), 1.18 (t, 3H).

Sources & evidence

ORD record
ord-488eccc0eb284ec9b9003d530c8f5912
Source dataset
uspto-grants-2007_05
Patent number
US07211668B2

Reaction notes

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