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HRID1349109

反应详情

EQUATION

反应方程式

HRID 1349109 的结构方程式

REACTANTS

反应物

3
结构：Nc1ccccc1N
HCID7243

1,2-Phenylenediamine

C6H8N2

结构：N#Cc1ccc(C(=O)Cl)cc1
HCID80172

4-Cyanobenzoyl chloride

C8H4ClNO

结构：CC(C)(C)OC(=O)N1CC(=CC#N)C[C@H]1C(=O)O
HCID69250314

未命名化合物

PRODUCTS

生成物

1
结构：N#CC=C1C[C@@H](c2nc3ccccc3[nH]2)N(C(=O)c2ccc(C#N)cc2)C1
HCID69247878

未命名化合物

PROCEDURE

实验过程

Following the general method as outlined in Example 22, starting from (2S,4EZ)-1-(tert-butoxycarbonyl)-4-(cyanomethylene)-2-pyrrolidinecarboxylic acid, 4-cyanobenzoyl chloride, and 1,2-benzenediamine the title compound was obtained in 84% purity by LC/MS. MS(ESI+): m/z=354.2.