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HRID 1349110作成日：2026年10月25日

3-Amino-9-ethylcarbazole → (2S,4EZ)-4-[(allyloxy)imino]-1-[4-(dimethylamino)butanoyl]-N-(9-ethyl-9H-carbazol-3-yl)-2-pyrrolidinecarboxamide

https://huagongshe.com/reaction/1349110

反応式

関与物質

役割名称HCID仕込み量
反応物3-Amino-9-ethylcarbazoleHCID 8588—
反応物4-(Dimethylamino)butanoyl chlorideHCID 15087690—
反応物(2S,4EZ)-4-[(allyloxy)imino)-1-(tert-butoxycarbonyl)-2-pyrrolidinecarboxylic acidHCID 58714562—
生成物(2S,4EZ)-4-[(allyloxy)imino]-1-[4-(dimethylamino)butanoyl]-N-(9-ethyl-9H-carbazol-3-yl)-2-pyrrolidinecarboxamideHCID 131725479—

反応手順

Following the general method as outlined in Example 22, starting from (2S,4EZ)-4-[(allyloxy)imino]-1-(tert-butoxycarbonyl)-2-pyrrolidinecarboxylic acid, 4-(dimethylamino)-butanoyl chloride and 9-ethyl-9H-carbazol-3-amine the title compound was obtained in 40% purity by LC/MS. MS(ESI+): m/z=490.4.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US07211601B2
出典データセットuspto-grants-2007_05
ORD IDord-d6f0d34ed7d84c3d9d2890f0a8627dd7
出典メモuspto-grants-2007_05