HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Tolyl isocyanate → HCID 69248876, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Tolyl isocyanate | HCID 69303 | — |
| Reactant | 3-Hydroxyazetidine | HCID 1514290 | — |
| Reactant | (2S)-1-(tert-butoxycarbonyl)-4-oxopyrrolidine-2-carboxylic acid | HCID 11593804 | — |
| Product | HCID 69248876 | HCID 69248876 | — |
Reaction Steps
Following the general method as outlined in Example 22, starting from 1-(tert-butoxycarbonyl)-4-oxoproline, 1-isocyanato-3-methylbenzene, and 3-azetidinol the title compound was obtained in 73% purity by LC/MS. MS(ESI+): m/z=318.0.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07211601B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-756cac0e47554cbca51c4095c721ab36 |
| Source note | uspto-grants-2007_05 |