N,N-Diethylethylenediamine → HCID 131725568, compound

HRID 1349225Notes

Reaction equation

HRID 1349225 reaction equation
C(OC([N:8]1[CH2:12][C:11](=[N:13][O:14][CH2:15][CH3:16])[CH2:10][C@H:9]1[C:17]([OH:19])=O)=O)(C)(C)C.[CH2:20]([N:22]([CH2:26][CH3:27])[CH2:23][CH2:24][NH2:25])[CH3:21]>>[CH2:20]([N:22]([CH2:26][CH3:27])[CH2:23][CH2:24][NH:25][C:17]([C@@H:9]1[CH2:10][C:11](=[N:13][O:14][CH2:15][CH3:16])[CH2:12][NH:8]1)=[O:19])[CH3:21]

Participants

3

Reactant 2

HCID 60993N,N-DiethylethylenediamineHCID 58714540(2S,4EZ)-1-(tertbutoxycarbonyl)-4-(ethoxyirnino)-2-pyrrolidinecarboxylic acid

Product 1

HCID 131725568HCID 131725568, compound

Procedure

Following the general method as outlined in Example 22, starting from (2S,4EZ)-1-(tert-butoxycarbonyl)-4-(ethoxyimino)-2-pyrrolidinecarboxylic acid, and N1,N1-diethyl-1,2-ethanediamine the title compound was obtained in 70% purity by LC/MS. (ESI+): m/z=271.0.

Sources & evidence

ORD record
ord-e24298e679844bdab8e03ddc1bd466ed
Source dataset
uspto-grants-2007_05
Patent number
US07211601B2

Reaction notes

Loading…