HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → HCID 10457089, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | p-Anisoyl chloride | HCID 7477 | — |
| Reactant | 4-(Dimethylamino)benzoyl chloride | HCID 4400782 | — |
| Reactant | HCID 10457089 | HCID 10457089 | — |
| Product | HCID 10457089 | HCID 10457089 | — |
| Product | HCID 86592032 | HCID 86592032 | — |
Reaction Steps
(±)-Cis-N-(4-chloro-phenyl)-N-[1-(4-methoxy-benzoyl)-2,7-dimethyl-1,2,3,4-tetrahydro-quinolin-4-yl]-acetamide was made following general procedure B, substituting 3-toluidine for aniline and 4-methoxybenzoyl chloride for 4-dimethylaminobenzoyl chloride. The reaction was non-selective and also (±)-cis-N-(4-chloro-phenyl)-N-[1-(4-methoxy-benzoyl)-2,5-dimethyl-1,2,3,4-tetrahydro-quinolin-4-yl]-acetamide was obtained in a 1:1 mixture with the titled compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07211672B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-3653278ae76640efbefc9dda453746af |
| Source note | uspto-grants-2007_05 |