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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1349720Generated: November 1, 2026

Triethylamine → HCID 22479700, compound

https://huagongshe.com/reaction/1349720

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTriethylamineHCID 8471—
ReactantMethoxyacetyl chlorideHCID 96623—
ReactantHCID 22480146HCID 22480146—
SolventTetrahydrofuranHCID 8028—
ProductHCID 22479700HCID 22479700—

Reaction Steps

The title compound was prepared using 3-(3-aminophenyl)-1-perhydro-2H-pyran-2-yl-1H-indazole-5-carbonitrile (0.150 g, 0.47 mmol) in tetrahydrofuran (5 mL), 2-methoxy acetyl chloride (0.086 mL, 0.94 mmol) and triethyl amine (0.327 mL, 2.35 mmol). The crude product was isolated after partition of the reaction mixture between ethyl acetate and water. The yield was not calculated: ES-MS (m/z) 391 [M+H]+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07211594B2
Source datasetuspto-grants-2007_05
ORD IDord-cf7213c646a54b2f8710c2500a2b1478
Source noteuspto-grants-2007_05