HCID 21094314, compound → HCID 21094313, compound

HRID 1350084Notes

Reaction equation

HRID 1350084 reaction equation
[N:1]([CH2:4][CH:5]1[C:14]2[C:9](=[CH:10][CH:11]=[C:12]([O:15][CH3:16])[CH:13]=2)[CH2:8][N:7]([C:17]([O:19][C:20]([CH3:23])([CH3:22])[CH3:21])=[O:18])[CH2:6]1)=[N+]=[N-]>CO.[Pd]>[NH2:1][CH2:4][CH:5]1[C:14]2[C:9](=[CH:10][CH:11]=[C:12]([O:15][CH3:16])[CH:13]=2)[CH2:8][N:7]([C:17]([O:19][C:20]([CH3:23])([CH3:22])[CH3:21])=[O:18])[CH2:6]1

Participants

4

Reactant 1

HCID 21094314HCID 21094314, compound

Product 1

HCID 21094313HCID 21094313, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 887MethanolSolvent

Procedure

The compound obtained in Step B (1.14 g) is dissolved in 100 ml of methanol and then palladium-on-carbon (120 mg) is added to the solution. The reaction mixture is stirred at ambient temperature and under hydrogen for 3 hours.

Sources & evidence

ORD record
ord-c5ffe9bca56b487f93cce321c19a247b
Source dataset
uspto-grants-2007_05
Patent number
US07214689B2

Reaction notes

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