N,N-Diethylethylenediamine → HCID 69507284, compound

HRID 1350184Notes

Reaction equation

HRID 1350184 reaction equation
[CH3:1][C:2]1[CH:6]=[C:5]([CH3:7])[NH:4][C:3]=1[C:8](=[C:12]1[C:20]2[C:15](=[CH:16][CH:17]=[CH:18][CH:19]=2)[NH:14][C:13]1=[O:21])[C:9](O)=[O:10].[CH2:22]([N:24]([CH2:28][CH3:29])[CH2:25][CH2:26][NH2:27])[CH3:23]>>[CH2:22]([N:24]([CH2:28][CH3:29])[CH2:25][CH2:26][NH:27][C:9](=[O:10])[C:8]([C:3]1[NH:4][C:5]([CH3:7])=[CH:6][C:2]=1[CH3:1])=[C:12]1[C:20]2[C:15](=[CH:16][CH:17]=[CH:18][CH:19]=2)[NH:14][C:13]1=[O:21])[CH3:23]

Participants

3

Reactant 2

HCID 60993N,N-DiethylethylenediamineHCID 69453471HCID 69453471, compound

Product 1

HCID 69507284HCID 69507284, compoundYield 46%

Procedure

(3,5-Dimethyl-1H-pyrrol-2-yl)-(2-oxo-1,2-dihydroindol-3-ylidene)-acetic acid (90 mg) was reacted with N,N-diethylethylenediamine (48 mg) using method B to give 37 mg (46%) of the title compound.

Sources & evidence

ORD record
ord-1d2c2cc8ee674f1d9f78f65debbd5414
Source dataset
uspto-grants-2007_05
Patent number
US07214700B2

Reaction notes

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