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HRID1350553

反应详情

EQUATION

反应方程式

HRID 1350553 的结构方程式

REACTANTS

反应物

3
结构：c1ccc2c(N3CCNCC3)cccc2c1
HCID1342

1-(Naphthalen-1-yl)piperazine

C14H16N2

结构：O=C1c2ccccc2C(=O)N1CCBr
HCID11325

1H-Isoindole-1,3(2H)-dione, 2-(2-bromoethyl)-

C10H8BrNO2

结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

PRODUCTS

生成物

1
结构：O=C1c2ccccc2C(=O)N1CCN1CCN(c2cccc3ccccc23)CC1
HCID21096932

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

CONDITIONS

反应条件

温度
90 °C

PROCEDURE

实验过程

A suspension of 1.17 g (5.52 mmol) of 1-(1-naphthyl)piperazine (Tetrahedron Letters, 1998, 39(15), 2219–2222), 0.99 g (7.15 mol) of potassium carbonate and 1.68 g (6.62 mmol) of 2-(2-bromoethyl)-1H-isoindole-1,3(2H)-dione in 15 ml of N,N-dimethylformamide is heated at 90° C. for 2 hours.