3-azido-N-(5-tert-butyl-3-methanesulfonylamino-2-methoxy-phenyl)-4-methyl-benzamide → HCID 21097153, compound

HRID 1350704Notes

Reaction equation

HRID 1350704 reaction equation
[N:1]([C:4]1[CH:5]=[C:6]([CH:27]=[CH:28][C:29]=1[CH3:30])[C:7]([NH:9][C:10]1[CH:15]=[C:14]([C:16]([CH3:19])([CH3:18])[CH3:17])[CH:13]=[C:12]([NH:20][S:21]([CH3:24])(=[O:23])=[O:22])[C:11]=1[O:25][CH3:26])=[O:8])=[N+:2]=[N-:3].[C:31]([S:35][C:36]1[N:37]([CH3:43])[C:38]([C:41]#[CH:42])=[CH:39][N:40]=1)([CH3:34])([CH3:33])[CH3:32]>>[C:16]([C:14]1[CH:13]=[C:12]([NH:20][S:21]([CH3:24])(=[O:22])=[O:23])[C:11]([O:25][CH3:26])=[C:10]([NH:9][C:7](=[O:8])[C:6]2[CH:27]=[CH:28][C:29]([CH3:30])=[C:4]([N:1]3[CH:42]=[C:41]([C:38]4[N:37]([CH3:43])[C:36]([S:35][C:31]([CH3:33])([CH3:32])[CH3:34])=[N:40][CH:39]=4)[N:3]=[N:2]3)[CH:5]=2)[CH:15]=1)([CH3:18])([CH3:19])[CH3:17]

Participants

3

Reactant 2

HCID 210792023-azido-N-(5-tert-butyl-3-methanesulfonylamino-2-methoxy-phenyl)-4-methyl-benzamideHCID 21097283HCID 21097283, compound

Product 1

HCID 21097153HCID 21097153, compound

Procedure

Example 30 was prepared from 3-azido-N-(5-tert-butyl-3-methanesulfonylamino-2-methoxy-phenyl)-4-methyl-benzamide and 2-tert-butylsulfanyl-5-ethynyl-1-methyl-1H-imidazole in the same manner as Example 15. ESI MS m/z 626 [C30H39N7O4S2+H]+.

Sources & evidence

ORD record
ord-b363d02ad9e5443193d57c458ea1410b
Source dataset
uspto-grants-2007_05
Patent number
US07214802B2

Reaction notes

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