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3-Azido-4-methylbenzoic acid → 3-Azido-N-(5-tert-butyl-3-methanesulfonylamino-2-methyl-phenyl)-4-methyl-benzamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-Azido-4-methylbenzoic acid | HCID 17973091 | — |
| 反応物 | 3-azido-N-(5-tert-butyl-3-methanesulfonylamino-2-methoxy-phenyl)-4-methyl-benzamide | HCID 21079202 | — |
| 反応物 | N-(3-Amino-5-tert-butyl-2-methyl-phenyl)-methanesulfonamide | HCID 21097367 | — |
| 生成物 | 3-Azido-N-(5-tert-butyl-3-methanesulfonylamino-2-methyl-phenyl)-4-methyl-benzamide | HCID 21097304 | — |
反応手順
3-Azido-N-(5-tert-butyl-3-methanesulfonylamino-2-methyl-phenyl)-4-methyl-benzamide was prepared from 3-azido-4-methyl benzoic acid (U.S. Ser. No. 04/102,492) and N-(3-Amino-5-tert-butyl-2-methyl-phenyl)-methanesulfonamide in the same manner as 3-azido-N-(5-tert-butyl-3-methanesulfonylamino-2-methoxy-phenyl)-4-methyl-benzamide (Example 15).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07214802B2 |
| 出典データセット | uspto-grants-2007_05 |
| ORD ID | ord-62ee222ff5df4e7eb73d3ba63f75ce7f |
| 出典メモ | uspto-grants-2007_05 |