o-Toluenesulfonyl chloride → 4-(4-Cyanophenyl)butyl toluenesulphonate

HRID 1351131Notes

Reaction equation

HRID 1351131 reaction equation
[C:1]1([CH3:11])[C:2]([S:7](Cl)(=[O:9])=[O:8])=[CH:3][CH:4]=[CH:5][CH:6]=1.[OH:12][CH2:13][CH2:14][CH2:15][CH2:16][C:17]1[CH:24]=[CH:23][C:20]([C:21]#[N:22])=[CH:19][CH:18]=1>>[C:1]1([CH3:11])[C:2]([S:7]([O:12][CH2:13][CH2:14][CH2:15][CH2:16][C:17]2[CH:18]=[CH:19][C:20]([C:21]#[N:22])=[CH:23][CH:24]=2)(=[O:9])=[O:8])=[CH:3][CH:4]=[CH:5][CH:6]=1

Participants

3

Reactant 2

HCID 8623o-Toluenesulfonyl chlorideHCID 185403804-(4-Hydroxybutyl)benzonitrile

Product 1

HCID 865936554-(4-Cyanophenyl)butyl toluenesulphonate

Procedure

The sub-title compound was prepared by addition of toluenesulphonyl chloride to 4-(4-hydroxybutyl)benzonitrile (see step (ii) above).

Sources & evidence

ORD record
ord-14aeed84e0124b3796c3e4e029b58bcf
Source dataset
uspto-grants-2007_05
Patent number
US07217708B2

Reaction notes

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