HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2-(4-Fluorophenyl)ethyl)(methyl)amine → 6-Methyl-7-oxo-4,5,6,7-tetrahydrobenzo[b]thiophene-3-sulfonic acid[2-(4-fluorophenyl)ethyl]-methyl-amide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2-(4-Fluorophenyl)ethyl)(methyl)amine | HCID 120234 | — |
| Reactant | 6-Methyl-7-oxo-4,5,6,7-tetrahydrobenzo[b]thiophene-3-sulfonyl chloride | HCID 21098672 | — |
| Product | 6-Methyl-7-oxo-4,5,6,7-tetrahydrobenzo[b]thiophene-3-sulfonic acid[2-(4-fluorophenyl)ethyl]-methyl-amide | HCID 21098670 | — |
Reaction Steps
From 6-methyl-7-oxo-4,5,6,7-tetrahydrobenzo[b]thiophene-3-sulfonyl chloride (the compound of Preparation Example 13) (140 mg) and [2-(4-fluorophenyl)ethyl]methylamine (the compound of Preparation Example 14) (98 mg), the title compound (152 mg) was obtained as an orange oily substance, in the same way as Preparation Example 41.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07217723B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-a71681e5cb1441d9880ce2217c7aaf53 |
| Source note | uspto-grants-2007_05 |