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HRID1351326

反应详情

EQUATION

反应方程式

HRID 1351326 的结构方程式

REACTANTS

反应物

1
结构：CN(CC(O)c1ccc(F)cc1)S(=O)(=O)c1csc2c1CCC/C2=N/O
HCID11350049

未命名化合物

PRODUCTS

生成物

1
结构：CN(CC(O)c1ccc(F)cc1)S(=O)(=O)c1csc2c1CCC/C2=N\O
HCID87825251

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCCCCC.CCOC(C)=O
溶剂HCID21226206

未命名化合物

PROCEDURE

实验过程

Among the reaction product from Example 1, those fractions from the fractionation by silica gel column chromatography (ethyl acetate/hexane) that are low polarity elution fractions (demonstrating high Rf value on TLC) were collected, and the title compound (29 mg) was obtained as a colorless solid.

WORKUP

后处理

  1. washpolarity elution fractions (demonstrating high Rf value on TLC)
  2. customwere collected