3,4-Dichlorobenzyl alcohol → HCID 17989819, compound

HRID 1351445Notes

Reaction equation

HRID 1351445 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([CH:7]=[CH:8][C:9]=1[Cl:10])[CH2:5][OH:6].Cl.[NH2:12][CH2:13][C:14](=[O:20])[CH2:15][CH2:16][C:17](O)=[O:18]>>[ClH:1].[NH2:12][CH2:13][C:14](=[O:20])[CH2:15][CH2:16][C:17]([O:6][CH2:5][C:4]1[CH:7]=[CH:8][C:9]([Cl:10])=[C:2]([Cl:1])[CH:3]=1)=[O:18]

Participants

3

Reactant 2

HCID 157283,4-Dichlorobenzyl alcoholHCID 123608Aminolevulinic Acid Hydrochloride

Product 1

HCID 17989819HCID 17989819, compound

Procedure

From 3,4-dichlorobenzyl alcohol (5.0 g; 28 mmol) and 5-amino-4-oxopentanoic acid hydrochloride (1.0 g; 6.0 mmol). The reaction was complete after 45 h at 100° C. The yield was 1.12 g (57%).

Sources & evidence

ORD record
ord-ef91362a2dab48a290f35e3b863ef189
Source dataset
uspto-grants-2007_05
Patent number
US07217736B2

Reaction notes

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