HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylbenzyl alcohol → 2-Methylbenzyl 5-aminolevulinate hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylbenzyl alcohol | HCID 6994 | — |
| Reactant | Aminolevulinic Acid Hydrochloride | HCID 123608 | — |
| Product | 2-Methylbenzyl 5-aminolevulinate hydrochloride | HCID 17989817 | — |
Reaction Steps
From 2-methylbenzyl alcohol (5.0 g; 41 mmol) and 5-amino-4-oxopentanoic acid hydrochloride (1.0 g; 6.0 mmol). The reaction was complete after 4 days at 100° C. The yield was 0.72 g (44%). Mp 107–109° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07217736B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-13c8fcfc957f4ceca92457f59328fdf7 |
| Source note | uspto-grants-2007_05 |