HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Alcohol → HCID 69425031, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Alcohol | HCID 244 | — |
| Reactant | 3,3-Dimethyl-1-butanol | HCID 12233 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 3-Fluorobenzylic alcohol | HCID 68008 | — |
| Reactant | HCID 69381055 | HCID 69381055 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 69425031 | HCID 69425031 | — |
Reaction Steps
Examples 362–368 were synthesized following the above mentioned procedure for example 359 using the intermediate (5-cyano-7-hydroxy-8-methyl-1-propyl-1,3,4,9-tetrahydro-pyrano[3,4-b]indol-1-yl)-acetic acid ethyl ester and coupling it with the following alcohols: ethanol, methanol, isopropanol, n-butyl alcohol, 3,3-dimethyl-1-butanol, 3-fluorobenzyl alcohol, and benzyl alcohol. The resulting esters were hydrolyzed using 10% NaOH (aq) in EtOH.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07217730B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-b41c4f9b49f744718f0f1d1e7f8beb95 |
| Source note | uspto-grants-2007_05 |