4-Aminophthalimide → HCID 17838186, compound

HRID 1352113Notes

Reaction equation

HRID 1352113 reaction equation
[NH2:1][C:2]1[CH:12]=[C:6]2[C:7]([NH:9][C:10](=[O:11])[C:5]2=[CH:4][CH:3]=1)=[O:8].[Cl:13][C:14]1[CH:19]=[C:18]([Cl:20])[CH:17]=[C:16]([Cl:21])[C:15]=1[N:22]=[C:23]=[O:24]>C1(C)C=CC=CC=1>[O:11]=[C:10]1[C:5]2[C:6](=[CH:12][C:2]([NH:1][C:23]([NH:22][C:15]3[C:16]([Cl:21])=[CH:17][C:18]([Cl:20])=[CH:19][C:14]=3[Cl:13])=[O:24])=[CH:3][CH:4]=2)[C:7](=[O:8])[NH:9]1

Participants

4

Reactant 2

HCID 729154-AminophthalimideHCID 6135742,4,6-Trichlorophenyl isocyanate

Product 1

HCID 17838186HCID 17838186, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Conditions

Temperature
110 °C

Procedure

5-Aminophthalimide (100 mg, 0.62 mmol) and 2,4,6-trichlorophenyl isocyanate (150.9 mg, 0.68 mmol) were dissolved in toluene, and the mixture was then stirred at 110° C. for 4 hr.

Sources & evidence

ORD record
ord-f9fa2f160a1c4ba38dec56460e7e702b
Source dataset
uspto-grants-2007_05
Patent number
US07217722B2

Reaction notes

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