Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | 2,6-Dichlorobenzothiazole | HCID 77176 | — |
| Solvent | Sulfuric Acid | HCID 1118 | — |
| Product | HCID 18916400 | HCID 18916400 | — |
Reaction Steps
4.76 g (23 mmol) of 2,6-dichlorobenzothiazole, in solution in 10 ml of concentrated sulphuric acid, are introduced into a 100 ml round-bottomed flask. The mixture is cooled to 17° C. in order to add a solution of 1.62 g (26 mmol) of nitric acid in 10 ml of sulphuric acid and then the temperature is allowed to rise to ambient temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07220740B2 |
|---|
| Source dataset | uspto-grants-2007_05 |
|---|
| ORD ID | ord-be8b690d45194f5a8e5afc8579bc51de |
|---|
| Source note | uspto-grants-2007_05 |
|---|
