HuagongsheHuagongshe Chemistry Print Report · For research reference only
Neopentyl alcohol → 2-(2,2-Dimethyl-propoxy)-5-methanesulfonyl-benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Neopentyl alcohol | HCID 6404 | — |
| Reactant | 2-Chloro-5-(methylsulphonyl)benzoic acid | HCID 2329132 | — |
| Product | 2-(2,2-Dimethyl-propoxy)-5-methanesulfonyl-benzoic acid | HCID 21100203 | — |
Reaction Steps
Prepared in analogy to Example A1 (b) from 2-chloro-5-methanesulfonyl-benzoic acid (Example A1(a)) and 2,2-dimethyl-propan-1-ol. The crude material was purified by preparative HPLC to yield the title compound as a white solid. MS (m/e): 285.1 ([M−H]−, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07220744B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-f085fec14ac748d995463b5766602f77 |
| Source note | uspto-grants-2007_05 |