2,2,3,3,3-Pentafluoropropanol → 5-Methanesulfonyl-2-(2,2,3,3,3-pentafluoro-propoxy)-benzoic acid

HRID 1352275Notes

Reaction equation

HRID 1352275 reaction equation
F[C:2]1[CH:10]=[CH:9][C:8]([S:11]([CH3:14])(=[O:13])=[O:12])=[CH:7][C:3]=1[C:4]([OH:6])=[O:5].[F:15][C:16]([F:23])([C:19]([F:22])([F:21])[F:20])[CH2:17][OH:18]>>[CH3:14][S:11]([C:8]1[CH:9]=[CH:10][C:2]([O:18][CH2:17][C:16]([F:23])([F:15])[C:19]([F:22])([F:21])[F:20])=[C:3]([CH:7]=1)[C:4]([OH:6])=[O:5])(=[O:13])=[O:12]

Participants

3

Reactant 2

HCID 98722,2,3,3,3-PentafluoropropanolHCID 224675662-Fluoro-5-methanesulfonyl-benzoic acid

Product 1

HCID 211003155-Methanesulfonyl-2-(2,2,3,3,3-pentafluoro-propoxy)-benzoic acid

Procedure

Prepared in analogy to Example A14(c) from 2-fluoro-5-methanesulfonyl-benzoic acid (Example A14(b)) and 2,2,3,3,3-pentafluoro-1-propanol. MS (m/e): 346.9 ([M−H]−, 100%)

Sources & evidence

ORD record
ord-d80dece3626248a6b2f6f1fe208435b3
Source dataset
uspto-grants-2007_05
Patent number
US07220744B2

Reaction notes

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