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HRID1352408

反应详情

EQUATION

反应方程式

HRID 1352408 的结构方程式

REACTANTS

反应物

2
结构：c1ccc(-c2nsc(N3CCNCC3)n2)cc1
HCID2777760

3-Phenyl-5-piperazino-1,2,4-thiadiazole

C12H14N4S

结构：CC(C)Oc1ccc(C#N)cc1C(=O)O
HCID21100297

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)Oc1ccc(C#N)cc1C(=O)N1CCN(c2nc(-c3ccccc3)ns2)CC1
HCID21100295

未命名化合物

收率 74%

PROCEDURE

实验过程

Prepared in analogy to example 1 (b) from 5-cyano-2-isopropoxy-benzoic acid (Example A28) and 3-phenyl-5-piperazino-1,2,4-thiadiazole. The crude material was purified by chromatography (SiO2, ethyl acetate/heptane) to yield the title compound as a white solid (yield 74%). MS (m/e): 434.1 (M+H+, 100%).

WORKUP

后处理

  1. customThe crude material was purified by chromatography (SiO2, ethyl acetate/heptane)