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Dabsyl chloride → n-{2-[2-(4-Amino-2,6,7-trimethyl-1h-imidazo[4,5-c]pyridin-1-yl)ethoxy]ethyl}-4-{[4-(dimethylamino)phenyl]diazenyl}benzenesulfonamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dabsyl chloride | HCID 91660 | — |
| 反応物 | 1-[2-(2-aminoethoxy)ethyl]-2,6,7-trimethyl-1H-imidazo[4,5-c]pyridin-4-amine | HCID 21913053 | — |
| 生成物 | n-{2-[2-(4-Amino-2,6,7-trimethyl-1h-imidazo[4,5-c]pyridin-1-yl)ethoxy]ethyl}-4-{[4-(dimethylamino)phenyl]diazenyl}benzenesulfonamide | HCID 10437562 | — |
反応手順
Using the method of Examples 34–50, 4-dimethylaminoazobenzene-4′-sulfonyl chloride was reacted with 1-[2-(2-aminoethoxy)ethyl]-2,6,7-trimethyl-1H-imidazo[4,5 -c]pyridin-4-amine to provide the desired compound. The product was purified using Method A. The observed accurate mass was 551.2551.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07220758B2 |
| 出典データセット | uspto-grants-2007_05 |
| ORD ID | ord-d3986250f4504e31af56d5794fe3f6dd |
| 出典メモ | uspto-grants-2007_05 |