4-Morpholinecarbonyl chloride → N-{2-[2-(4-amino-2,6,7-trimethyl-1H-imidazo[4,5-c]pyridin-1-yl)ethoxy]ethyl}morpholine-4-carboxamide

Participants

Role	Name	HCID	Charge
Reactant	4-Morpholinecarbonyl chloride	HCID 84810	—
Reactant	1-[2-(2-aminoethoxy)ethyl]-2,6,7-trimethyl-1H-imidazo[4,5-c]pyridin-4-amine	HCID 21913053	—
Product	N-{2-[2-(4-amino-2,6,7-trimethyl-1H-imidazo[4,5-c]pyridin-1-yl)ethoxy]ethyl}morpholine-4-carboxamide	HCID 10022418	—

Reaction Steps

Using the method of Examples 54–68, 4-morpholinecarbonyl chloride was reacted with 1-[2-(2-aminoethoxy)ethyl]-2,6,7-trimethyl-1H-imidazo[4,5-c]pyridin-4-amine to provide the desired compound. The product was purified using Method A. The observed accurate mass was 377.2295.

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US07220758B2
Source dataset	uspto-grants-2007_05
ORD ID	ord-59fd0410bd08427690ca86da35af4c6b
Source note	uspto-grants-2007_05