HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Amino-1-propanol → HCID 21913176, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Amino-1-propanol | HCID 9086 | — |
| Reactant | 2,4-Dichloro-5,6-dimethyl-3-nitropyridine | HCID 12109123 | — |
| Product | HCID 21913176 | HCID 21913176 | 59.1% |
Reaction Steps
Using the general method of Example 89 Part A, 3-aminopropan-1-ol (9.52 mL, 124 mmol) was reacted with 2,4-dichloro-5,6-dimethyl-3-nitropyridine (25 g, 113 mmol) to provide 17.35 g of 3-[(2-chloro-5,6-dimethyl-3-nitropyridin-4-yl)amino]propan-1-ol as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07220758B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-02f4db533faa4b5f926e186bce48aa02 |
| Source note | uspto-grants-2007_05 |