HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 86585868, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 3,6-Dichloropyridazine | HCID 67331 | — |
| Reactant | HCID 53849828 | HCID 53849828 | — |
| Product | HCID 86585868 | HCID 86585868 | — |
Reaction Steps
The title compound was prepared according to Preparation 3 with 3,6-dichloropyridazine and (7R,9aS)-7-(4-fluorophenoxy)methyl-2,3,4,6,7,8,9,9a-octahydro-1H-pyrido[1,2-a]pyrazine. mp (.HCl) 265–270° C. 13C NMR (base, CDCl3): δ 26.8, 29.0, 36.4, 45.1, 50.4, 54.4, 58.6, 60.3, 71.5, 115.2, 115.3, 115.4, 115.6, 115.9, 128.7, 146.7, 155.0, 155.6, 158.76, 158.82. HRMS calcd for C19H22ClFN4O: 376.1461; found: 376.1453.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07220753B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-bebd82f7d80a4d4b8f66a044bc608027 |
| Source note | uspto-grants-2007_05 |